反応式
[CH2:1]=[O:2].[O:3]=[C:4]1[CH:11]2[CH2:12][CH:7]3[CH2:8][CH:9]([CH2:13][CH:5]1[CH:6]3O)[CH2:10]2.[ClH:15]>>[Cl:15][CH2:1][O:2][CH:10]1[CH:11]2[CH2:12][CH:7]3[CH2:6][CH:5]([CH2:13][CH:9]1[CH2:8]3)[C:4]2=[O:3]参加物
4
実験手順
Paraformaldehyde was added to 4-oxo-2-hydroxyadamantane, and a hydrogen chloride gas was injected at 2.5 equivalent amounts per this 4-oxo-2-hydroxyadamantane. Then, the reaction was conducted at a temperature of 50° C. for 12 hours. After the completion of the reaction, the product was distillated under reduced pressure so as to obtain 4-oxo-2-adamantyl chloromethyl ether (compound 1) represented by the following chemical formula (58).
後処理
- customAfter the completion of the reaction
出典と根拠
- ORDレコード
- ord-de9da7268278471faa1a361f851be596
- 出典データセット
- uspto-grants-2010_05
- 特許番号
- US07723007B2
関連ノート
読み込み中…