1-Butanol → HCID 178492027、化合物
反応式
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([NH:9][NH:10][C:11](=[S:13])[NH2:12])=[CH:5][CH:4]=1.[C:14](O)(=O)C.C(=N)N.C(O)CCC.O(C(C)C)C(C)C>O>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([N:9]2[CH:14]=[N:12][C:11]([SH:13])=[N:10]2)=[CH:7][CH:8]=1参加物
6
実験手順
A mixture of 10 parts of 2-(4-methoxyphenyl)hydrazinecarbothioamide, 10.6 parts of methanimidamide acetate and 80 parts of 1-butanol is stirred and refluxed for 1 hour. After cooling, water and 2,2'-oxybispropane are added, whereupon the product is precipitated. It is filtered off and dried, yielding 7.6 parts (73%) of 1-(4-methoxyphenyl)-1H-1,2,4-triazole-3-thiol.
後処理
- temperaturerefluxed for 1 hour
- temperatureAfter cooling
- customis precipitated
- filtrationIt is filtered off
- customdried
出典と根拠
- ORDレコード
- ord-7601420a85cb455da544bd47f10d3da5
- 出典データセット
- uspto-grants-1980_11
- 特許番号
- US04232034
反応ノート
読み込み中…