Azobisisobutyronitrile → Methyl Methacrylate

HRID 224763

反応式

HRID 224763 の反応式
[CH2:1]([N:3]([CH2:6][CH2:7][O:8][C:9](=[O:12])[CH:10]=[CH2:11])[CH2:4][CH3:5])[CH3:2].[CH2:13](OC(=O)C(C)=C)CCCCCCCCCCCCCCCCC.[CH3:37][O:38][C:39](=[O:43])[C:40]([CH3:42])=[CH2:41].CC(N=NC(C#N)(C)C)(C#N)C>C1C=CC=CC=1>[CH2:1]([N:3]([CH2:6][CH2:7][O:8][C:9](=[O:12])[C:10]([CH3:13])=[CH2:11])[CH2:4][CH3:5])[CH3:2].[CH3:37][O:38][C:39](=[O:43])[C:40]([CH3:42])=[CH2:41]

参加物

7

反応物 4

HCID 6547AzobisisobutyronitrileHCID 6658Methyl MethacrylateHCID 170502-(Diethylamino)ethyl acrylateHCID 122600Stearyl methacrylate

生成物 2

HCID 6658Methyl MethacrylateHCID 61012Diethylaminoethyl Methacrylate

試薬・触媒・溶媒 1

HCID 241Benzene溶媒

実験手順

A copolymer of 2-(N',N'-diethylamino)ethylmethacrylate, stearylmetacrylate, and methylmethacrylate was prepared by charging 0.048 mole of 2-(N',N'-diethylamino)ethylacrylate, 0.002 moles of stearylmethacrylate and 0.15 moles of methylmethacrylate in a retort containing 0.002 moles of AIBN. The retort had in accordance with Example 1 been gassed with nitrogen gas for half an hour before charging. The components were dissolved in dry benzene.

後処理

  1. waitbeen gassed with nitrogen gas for half an hour

出典と根拠

ORDレコード
ord-a8b5c3de89444517adf150eafbb00e2e
出典データセット
uspto-grants-1980_11
特許番号
US04234565

関連ノート

読み込み中…