Thionyl Chloride → HCID 10799500、化合物

HRID 2254403ノート

反応式

HRID 2254403 の反応式
[CH2:1]([C:9]1[CH:10]=[C:11]([CH:14]=[CH:15][CH:16]=1)[CH2:12]O)[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.S(Cl)([Cl:19])=O>C(Cl)(Cl)Cl>[CH2:1]([C:9]1[CH:10]=[C:11]([CH:14]=[CH:15][CH:16]=1)[CH2:12][Cl:19])[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

参加物

4

反応物 2

HCID 24386Thionyl ChlorideHCID 10488743Benzenemethanol, 3-(2-phenylethyl)-

生成物 1

HCID 10799500HCID 10799500、化合物収率 99%

試薬・触媒・溶媒 1

HCID 6212Chloroform溶媒

実験手順

The resulting alcohol (140 mg) was dissolved in 1 ml of chloroform, and 0.3 ml of thionyl chloride was added. The mixture was reacted at room temperature for 30 minutes. The reaction mixture was evaporated under reduced pressure to give 150 mg (yield 99%) of 3-phenethylbenzyl chloride as a pale yellow oil.

後処理

  1. customThe mixture was reacted at room temperature for 30 minutes
  2. customThe reaction mixture was evaporated under reduced pressure

出典と根拠

ORDレコード
ord-e0d091f11e3940e6979b2fad10b58995
出典データセット
uspto-grants-1993_08
特許番号
US05234946

反応ノート

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