ホームMCPワークベンチSkills
ホームワークベンチ通知マイページ
llms.txt · MCPガイドプライバシーポリシー · 利用規約 · サポートv1.8.0
  1. ホーム
  2. /反応

Acetonitrile → Ethyl 2-(4-benzyloxyphenyl)-5,6-dimethoxy-4,7-dioxo-2-indancarboxylate

HRID 2268520
ノート
印刷プレビュー

反応式

HRID 2268520 の反応式
O=[N+]([O-])[O-].[O-][N+](=O)[O-].[O-][N+](=O)[O-].[O-][N+](=O)[O-].[O-][N+](=O)[O-].[O-][N+](=O)[O-].[Ce+4].[NH4+].[NH4+].C(#N)C.[CH2:31]([O:38][C:39]1[CH:44]=[CH:43][C:42]([C:45]2([C:62]([O:64][CH2:65][CH3:66])=[O:63])[CH2:53][C:52]3[C:47](=[C:48]([O:60]C)[C:49]([O:58][CH3:59])=[C:50]([O:56][CH3:57])[C:51]=3[O:54]C)[CH2:46]2)=[CH:41][CH:40]=1)[C:32]1[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=1>O>[CH2:31]([O:38][C:39]1[CH:40]=[CH:41][C:42]([C:45]2([C:62]([O:64][CH2:65][CH3:66])=[O:63])[CH2:46][C:47]3[C:48](=[O:60])[C:49]([O:58][CH3:59])=[C:50]([O:56][CH3:57])[C:51](=[O:54])[C:52]=3[CH2:53]2)=[CH:43][CH:44]=1)[C:32]1[CH:33]=[CH:34][CH:35]=[CH:36][CH:37]=1
参加物実験手順後処理出典と根拠反応ノート

参加物

5

反応物 3

HCID 6342AcetonitrileHCID 180504Ceric ammonium nitrateHCID 18348586Ethyl 2-(4-benzyloxyphenyl)-4,5,6,7-tetramethoxy-2-indancarboxylate

生成物 1

HCID 15552353Ethyl 2-(4-benzyloxyphenyl)-5,6-dimethoxy-4,7-dioxo-2-indancarboxylate収率 54.1%

試薬・触媒・溶媒 1

HCID 962Water溶媒2 回

実験手順

A water (1.0 ml) solution of CAN (976 mg, 1.78 mmols) was dropwise added to an acetonitrile (7.0 ml) solution of ethyl 2-(4-benzyloxyphenyl)-4,5,6,7-tetramethoxy-2-indancarboxylate (350 mg, 0.711 mmols) with cooling with ice and stirring was continued for 15 minutes. Water was added to the reaction mixture, which was then extracted with ethyl acetate. The organic layer was washed with water and a saturated aqueous sodium chloride solution, and then dried. The solvent was evaporated in vacuo, and the resulting crude product was purified by silica gel column chromatography (hexane:ethyl acetate=5:1) followed by recrystallization from hexane-ethyl acetate to obtain the entitled compound (178 mg) as crystals.

後処理

  1. temperaturewith cooling with ice
  2. extractionwas then extracted with ethyl acetate
  3. washThe organic layer was washed with water
  4. dry with materiala saturated aqueous sodium chloride solution, and then dried
  5. customThe solvent was evaporated in vacuo
  6. customthe resulting crude product was purified by silica gel column chromatography (hexane:ethyl acetate=5:1)
  7. customfollowed by recrystallization from hexane-ethyl acetate

出典と根拠

ORDレコード
ord-3af06506c80f456ba4a389ae5b5055a9
出典データセット
uspto-grants-2001_12
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US06326369B1

反応ノート

読み込み中…

このページの内容参加物実験手順後処理出典と根拠反応ノート