反応式
[NH2:1][C:2]1[C:7]([O:8][CH2:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[CH:6][CH:5]=[CH:4][N:3]=1.[CH:16]1([N+:22]#[C-:23])[CH2:21][CH2:20][CH2:19][CH2:18][CH2:17]1.[C:24]([NH:27][C:28]1[CH:35]=[CH:34][C:31]([CH:32]=O)=[CH:30][CH:29]=1)(=[O:26])[CH3:25]>Cl(O)(=O)(=O)=O>[CH2:9]([O:8][C:7]1[C:2]2[N:3]([C:23]([NH:22][CH:16]3[CH2:21][CH2:20][CH2:19][CH2:18][CH2:17]3)=[C:32]([C:31]3[CH:34]=[CH:35][C:28]([NH:27][C:24](=[O:26])[CH3:25])=[CH:29][CH:30]=3)[N:1]=2)[CH:4]=[CH:5][CH:6]=1)[C:10]1[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=1参加物
5
実験手順
Compound (7) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-3-benzyloxypyridine solution (0.1 M, DCM), 0.575 ml of cyclohexyl isocyanide solution (0.2 M, DCM), 0.500 ml of 4-acetamidobenzaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
出典と根拠
- ORDレコード
- ord-f941adf25dc84ba8b696c02443532c05
- 出典データセット
- uspto-grants-2005_02
- 特許番号
- US06849642B2
関連ノート
読み込み中…