Acetophenone → N-(1-phenylethyl)formamide
反応式
[CH:1]([O-:3])=O.[NH4+:4].[C:5]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)(=O)[CH3:6]>C(O)=O>[CH:1]([NH:4][CH:5]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)[CH3:6])=[O:3]参加物
4
実験手順
In the same manner as in Example 1 except that a mixture of formic acid, ammonium formate and acetophenone was heated with stirring at 160° C. for 6 hours in place of the concurrent addition of acetophenone and formic acid to ammonium formate for 3 hours and keeping the mass after the addition stirred for 3 hours, the reaction and post treatment were carried out to obtain 112 g of crude N-formyl-1-phenylethylamine; the purity: 82.7%.
後処理
- temperaturewas heated
- additionafter the addition
- customthe reaction and post treatment
出典と根拠
- ORDレコード
- ord-8468a00c9f9943b183cfdddcc8e40cb4
- 出典データセット
- uspto-grants-2000_07
- 特許番号
- US06093851
反応ノート
読み込み中…