Sodium Hydroxide → (2-Bromophenyl)hydrazine

HRID 2360490

反応式

HRID 2360490 の反応式
Cl.[Br:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[NH:9][NH2:10].[OH-].[Na+]>C1(C)C=CC=CC=1>[Br:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[NH:9][NH2:10]

参加物

4

反応物 2

HCID 14798Sodium HydroxideHCID 27239122-Bromophenylhydrazine hydrochloride

生成物 1

HCID 85583(2-Bromophenyl)hydrazine

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

15 g 2-bromophenylhydrazine hydrochloride are suspended in 400 ml of toluene and combined with 240 ml of 1 N sodium hydroxide solution. The mixture is stirred for 1 hour and the phases are separated. The organic phase is dried on magnesium sulphate and the solvents are eliminated in vacuo. The crude product thus obtained is further reacted directly.

後処理

  1. customthe phases are separated
  2. customThe organic phase is dried on magnesium sulphate

出典と根拠

ORDレコード
ord-15172afbc4084c749fa1d4454ea24d19
出典データセット
uspto-grants-2014_04
特許番号
US08686022B2

関連ノート

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