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Triethylamine → HCID 12115478、化合物

HRID 2373329
ノート
印刷プレビュー

反応式

HRID 2373329 の反応式
[Cl:1][C:2]1[N:6]([CH3:7])[N:5]=[C:4]([C:8]([F:11])([F:10])[F:9])[C:3]=1[C:12]([OH:14])=O.[CH3:15][CH:16]([C:21]1[CH:27]=[C:26]([CH:28]([C:33]([F:36])([F:35])[F:34])[C:29]([F:32])([F:31])[F:30])[CH:25]=[CH:24][C:22]=1[NH2:23])[CH2:17][CH:18]([CH3:20])[CH3:19].C(N(CC)CC)C>S(Cl)(Cl)=O.O1CCCC1.C(OCC)(=O)C>[CH3:15][CH:16]([C:21]1[CH:27]=[C:26]([CH:28]([C:29]([F:31])([F:32])[F:30])[C:33]([F:34])([F:35])[F:36])[CH:25]=[CH:24][C:22]=1[NH:23][C:12]([C:3]1[C:4]([C:8]([F:11])([F:10])[F:9])=[N:5][N:6]([CH3:7])[C:2]=1[Cl:1])=[O:14])[CH2:17][CH:18]([CH3:19])[CH3:20]
参加物実験手順後処理出典と根拠反応ノート

参加物

7

反応物 3

HCID 8471TriethylamineHCID 27738065-Chloro-1-Methyl-3-(Trifluoromethyl)-1H-Pyrazole-4-Carboxylic AcidHCID 12115477HCID 12115477、化合物

生成物 1

HCID 12115478HCID 12115478、化合物収率 43.3%

試薬・触媒・溶媒 3

HCID 8028Tetrahydrofuran溶媒HCID 8857
Ethyl Acetate
溶媒
HCID 24386Thionyl Chloride溶媒

実験手順

5-Chloro-1-methyl-3-trifluoromethylpyrazole-4-carboxylic acid (230 mg, 1 mmol) was dissolved in thionyl chloride (2 ml), and the solution was stirred at reflux temperature for 2 hours. After concentration under reduced pressure, the resulting acid chloride was added to a solution of 2-(1,3-dimethylbutyl)-4-[2,2,2-trifluoro-1-(trifluoromethyl)ethyl]aniline (330 mg, 1 mmol) and triethylamine (150 mg, 1.5 mmol) in tetrahydrofuran (10 ml) under ice-cooling, and the resulting mixture was stirred at room temperature for 2 hours. The reaction mixture was diluted with ethyl acetate and then washed with water. The organic layer was dried over anhydrous magnesium sulfate and then concentrated under reduced pressure, and the resulting residue was separated and purified by silica gel column chromatography (hexane:ethyl acetate=3:1) to obtain 233 mg of the desired compound.

後処理

  1. temperatureat reflux temperature for 2 hours
  2. concentrationAfter concentration under reduced pressure
  3. temperaturecooling
  4. stirringthe resulting mixture was stirred at room temperature for 2 hours
  5. washwashed with water
  6. dry with materialThe organic layer was dried over anhydrous magnesium sulfate
  7. concentrationconcentrated under reduced pressure
  8. customthe resulting residue was separated
  9. custompurified by silica gel column chromatography (hexane:ethyl acetate=3:1)

出典と根拠

ORDレコード
ord-f97285f705ca4013b165a1494cc99cab
出典データセット
uspto-grants-2008_12
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US07459477B2

反応ノート

読み込み中…

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