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3-Pyridinemethanamine → 5-(5-benzyl-1H-1,2,4-triazol-3-yl)-3-methyl-N-(pyridin-3-ylmethyl)thiophene-2-carboxamide

HRID 2381861
ノート
印刷プレビュー

反応式

HRID 2381861 の反応式
[CH2:1]([C:8]1[NH:12][N:11]=[C:10]([C:13]2[S:17][C:16]([C:18]([OH:20])=O)=[C:15]([CH3:21])[CH:14]=2)[N:9]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.ON1C2C=CC=CC=2N=N1.Cl.C(N=C=NCCCN(C)C)C.C(N(CC)C(C)C)(C)C.[NH2:53][CH2:54][C:55]1[CH:56]=[N:57][CH:58]=[CH:59][CH:60]=1>CN(C)C=O.C(OCC)(=O)C>[CH2:1]([C:8]1[NH:12][N:11]=[C:10]([C:13]2[S:17][C:16]([C:18]([NH:53][CH2:54][C:55]3[CH:56]=[N:57][CH:58]=[CH:59][CH:60]=3)=[O:20])=[C:15]([CH3:21])[CH:14]=2)[N:9]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1
参加物実験手順後処理出典と根拠反応ノート

参加物

8

反応物 5

HCID 310183-PyridinemethanamineHCID 757711-HydroxybenzotriazoleHCID 81531DiisopropylethylamineHCID 27239391,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochlorideHCID 591797135-(5-benzyl-1H-1,2,4-triazol-3-yl)-3-methylthiophene-2-carboxylic acid

生成物 1

HCID 24957855
5-(5-benzyl-1H-1,2,4-triazol-3-yl)-3-methyl-N-(pyridin-3-ylmethyl)thiophene-2-carboxamide
収率 67%

試薬・触媒・溶媒 2

HCID 6228Dimethylformamide溶媒HCID 8857Ethyl Acetate溶媒

実験手順

To a stirred mixture of 5-(5-benzyl-1H-1,2,4-triazol-3-yl)-3-methylthiophene-2-carboxylic acid (0.13 g, 0.43 mmol), 1-hydroxybenzotriazole (0.088 g, 0.65 mmol) and 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride (0.13 g, 0.65 mmol) in anhydrous N,N-dimethylformamide (2 mL) was added N,N-diisopropylethylamine (0.23 mL, 1.30 mmol), followed by the addition of 3-(aminomethyl)pyridine (0.044 mL, 0.44 mmol). The resulting reaction mixture was stirred at ambient temperature for 18 h, and diluted with ethyl acetate (75 mL). The organic layer was washed with saturated aqueous sodium bicarbonate (3×35 mL) and water (35 mL), dried over sodium sulfate, filtered and concentrated in vacuo. The residue was purified by column chromatography eluted with 10% methanol in dichloromethane to afford the title compound as a colorless foam (0.11 g, 67%): mp 82° C. (dec.); 1H NMR (300 MHz, DMSO-d6) δ 8.66 (t, J=5.6 Hz, 1H), 8.55 (s, 1H), 8.46 (s, 1H), 7.73 (d, J=7.9 Hz, 1H), 7.42-7.20 (m, 8H), 4.44 (d, J=5.6 Hz, 2H), 4.10 (s, 2H), 2.43 (s, 3H); MS (ES+) m/z 390.3 (M+1).

後処理

  1. customThe resulting reaction mixture
  2. washThe organic layer was washed with saturated aqueous sodium bicarbonate (3×35 mL) and water (35 mL)
  3. dry with materialdried over sodium sulfate
  4. filtrationfiltered
  5. concentrationconcentrated in vacuo
  6. customThe residue was purified by column chromatography
  7. washeluted with 10% methanol in dichloromethane

出典と根拠

ORDレコード
ord-24cfe45382cd44768457ff343c84c569
出典データセット
uspto-grants-2012_09
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US08258160B2

反応ノート

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