Methyl iodide → HCID 12493310、化合物

HRID 2419642

反応式

HRID 2419642 の反応式
[N:1]1[CH:2]=[CH:3][N:4]2[C:9]=1[CH:8]=[N:7][NH:6][C:5]2=[S:10].[Na].[CH3:12]I>C(O)C>[CH3:12][S:10][C:5]1[N:4]2[CH:3]=[CH:2][N:1]=[C:9]2[CH:8]=[N:7][N:6]=1

参加物

5

反応物 3

HCID 6328Methyl iodideHCID 5360545SodiumHCID 12493308Imidazo[1,2-d]-as-triazine-5(6H)-thione

生成物 1

HCID 12493310HCID 12493310、化合物

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒2 回

実験手順

A 66.7 gm. portion of imidazo[1,2-d]-as-triazine-5(6H)-thione is added to 250 ml. of ethanol. A solution of 10.1 gm. of sodium reacted in 250 ml. of ethanol is added with swirling. A 27.7 ml. portion of methyl iodide is added slowly with swirling. The mixture is stored in a chillroom overnight, filtered and dried giving 56.5 gm. of the desired final product, m.p. 147°-149° C.

後処理

  1. customis stored in a chillroom overnight
  2. filtrationfiltered
  3. customdried
  4. customgiving 56.5 gm

出典と根拠

ORDレコード
ord-ede1b65fcce7417db802e0a7b4ea8876
出典データセット
uspto-grants-1978_08
特許番号
US04107309

関連ノート

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