Sodium Carbonate → HCID 20163824、化合物

HRID 256461ノート

反応式

HRID 256461 の反応式
C(=O)([O-])[O-].[Na+].[Na+].Cl.[NH2:8][OH:9].[CH2:10]([C:22]1[CH:29]=[CH:28][C:25]([CH2:26]Cl)=[CH:24][CH:23]=1)[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]>CN(C)C=O>[CH2:10]([C:22]1[CH:29]=[CH:28][C:25]([CH2:26][N:8]([CH2:26][C:25]2[CH:28]=[CH:29][C:22]([CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21])=[CH:23][CH:24]=2)[OH:9])=[CH:24][CH:23]=1)[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]

参加物

5

反応物 3

HCID 10340Sodium CarbonateHCID 443297Hydroxyamine hydrochlorideHCID 143857281-(Chloromethyl)-4-dodecylbenzene

生成物 1

HCID 20163824HCID 20163824、化合物

試薬・触媒・溶媒 1

HCID 6228Dimethylformamide溶媒

実験手順

The procedure of Example 1 is repeated using 16.0 g of sodium carbonate, 2.57 g of hydroxylamine hydrochloride and 21.83 g of p-dodecylbenzyl chloride in 75 ml of dimethylformamide kept at 50°-55° C. overnight under nitrogen. The product is isolated as a light brown oil.

後処理

  1. customThe product is isolated as a light brown oil

出典と根拠

ORDレコード
ord-99fb2909f79445eead3763d08521b4d9
出典データセット
uspto-grants-1987_10
特許番号
US04703073

反応ノート

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