Cyclohexanone → Prop-2-enenitrile--ethenylbenzene (1/1)
反応式
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][N:2]=1.C1(=O)CCCCC1>CN1CCCC1=O.[Cu]I>[CH2:9]=[CH:10][C:1]#[N:2].[CH2:3]=[CH:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1参加物
5
実験手順
A solution of 2.0 g. CuI, 1.4 g. isoquinoline (1:1 ratio), 50.0 g. N-methylpyrrolidone solvent, 46.6 g. cyclohexanone and 0.20 g. Lustran SAN 31-1,000 (10% on CuI) was prepared. The resulting coating solution was coated on 7 mil raw PET with number 10 Meyer rod and dried three minutes at 240° F. The coating had very good uniformity and clarity and was gold and blue iridescent and lustrous. The resistivity measured 13-20×107 Ω/sq. The solution after time showed some precipitation, which crystals were redissolved upon reheating.
後処理
- customdried three minutes at 240° F
- customsome precipitation, which crystals
- dissolutionwere redissolved
出典と根拠
- ORDレコード
- ord-3110b0bfc3814e4280160de68cfb5d7b
- 出典データセット
- uspto-grants-1993_11
- 特許番号
- US05259992
反応ノート
読み込み中…