反応式
[CH3:1][C:2]1([CH3:18])[CH:11]=[C:10]([CH3:12])[C:9]2[C:4](=[CH:5][CH:6]=[C:7]([C:13]3[CH:17]=[CH:16][S:15][CH:14]=3)[CH:8]=2)[NH:3]1.C1C(=O)N(Br)C(=O)C1.[CH2:27]([SH:30])[CH:28]=[CH2:29]>>[CH2:27]([S:30][CH2:12][C:10]1[C:9]2[C:4](=[CH:5][CH:6]=[C:7]([C:13]3[CH:17]=[CH:16][S:15][CH:14]=3)[CH:8]=2)[NH:3][C:2]([CH3:18])([CH3:1])[CH:11]=1)[CH:28]=[CH2:29]参加物
4
実験手順
2,2,4-Trimethyl-6-thiophen-3-yl-1,2-dihydroquinoline was brominated with NBS using the procedure described in Example 1 and then coupled with allyl mercaptan using the procedure described in Example 2 to provide 22 mg of the title compound as a oil.
出典と根拠
- ORDレコード
- ord-2ae737324b1e4979a5f2376838cc0e72
- 出典データセット
- uspto-grants-2005_02
- 特許番号
- US06858627B2
関連ノート
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