Water → Isodecyl acrylate
反応式
[CH2:1]([OH:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH:8]([CH3:10])[CH3:9].[CH3:12][C:13]1[CH:14]=CC(S(O)(=O)=O)=CC=1.[OH2:23]>C1(C)C(C)=CC=CC=1>[C:12]([O:11][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH:8]([CH3:9])[CH3:10])(=[O:23])[CH:13]=[CH2:14]参加物
5
反応条件
- 温度
- 140 °C
実験手順
To 157 g isodecyl alcohol in 200 ml xylene is added 117 g AA, 1.0 g HQ and 2.0Q PTSA. The reaction mixture is heated for 2 hrs. at reflux (140° C) while the water of reaction is collected (17 ml). The reaction mixture is cooled and the xylene removed under reduced pressure to give 250 g isodecyl acrylate. The analytical data for this acrylate is shown below.
後処理
- temperatureThe reaction mixture is heated for 2 hrs
- customis collected (17 ml)
- temperatureThe reaction mixture is cooled
- customthe xylene removed under reduced pressure
出典と根拠
- ORDレコード
- ord-7aeb45784b7e46019546e24d9d59e0ae
- 出典データセット
- uspto-grants-1977_07
- 特許番号
- US04035409
反応ノート
読み込み中…