Hydrochloric Acid → 2-Propenoic acid, 3-phenyl-

HRID 259636

反応式

HRID 259636 の反応式
[OH-:1].[Na+].Cl.[CH:4]1[CH:5]=[CH:6][C:7]2[C:13](C3C=CC(O)=CC=3)(C3C=CC(O)=CC=3)OC(=O)[C:8]=2[CH:9]=1.[CH2:28]([OH:30])[CH3:29]>>[CH:29]([C:28]([OH:1])=[O:30])=[CH:13][C:7]1[CH:8]=[CH:9][CH:4]=[CH:5][CH:6]=1

参加物

5

反応物 4

HCID 313Hydrochloric AcidHCID 702EthanolHCID 4764PhenolphthaleinHCID 14798Sodium Hydroxide

生成物 1

HCID 87842-Propenoic acid, 3-phenyl-

実験手順

Titration was effected by suspending the product (0.500g) in 95% ethanol (50 ml.) adding 0.5M sodium hydroxide (50 ml.), warming the mixture to reflux, cooling and back titrating with 0.5M hydrochloric acid using phenolphthalein as the indicator; it was found that 47.12 ml. of acid were required for neutralisation indicating 2.88 m.mole carboxyl/g of polymer.

後処理

  1. temperaturewarming the mixture
  2. temperatureto reflux
  3. temperaturecooling

出典と根拠

ORDレコード
ord-54112e168c8b43059d5bfa4cb18dd97e
出典データセット
uspto-grants-1977_07
特許番号
US04038469

関連ノート

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