反応式
[CH2:1]=[C:2]1[C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=2[CH:6]=[CH:5][N:4]2[C:13]([S:16][CH3:17])=[N:14][N:15]=[C:3]12.ClC1C=CC=C(C(OO)=[O:26])C=1>>[CH2:1]=[C:2]1[C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=2[CH:6]=[CH:5][N:4]2[C:13]([S:16]([CH3:17])=[O:26])=[N:14][N:15]=[C:3]12参加物
3
実験手順
By a procedure similar to that of Example 17, the reaction of 11-methylene-3-methylthio-11H-s-triazolo[3,4-b][3]benzazepine with m-chloroperbenzoic acid gave 11-methylene-3-methylsulfinyl-11H-s-triazolo[3,4-b][3]benzazepine as crystals. Recrystallization from ethyl acetate yielded colorless prisms, m.p. 140°-142° C.
出典と根拠
- ORDレコード
- ord-9ffaacf5506e43fda0f716845647efb3
- 出典データセット
- uspto-grants-1979_04
- 特許番号
- US04150139
関連ノート
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