1-Methylimidazole → HCID 178443590、化合物
反応式
[CH3:1][N:2]1[CH:6]=[CH:5][N:4]=[CH:3]1.[CH2:7]([Br:15])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]>C(O)C>[Br-:15].[CH2:7]([N+:4]1[CH:5]=[CH:6][N:2]([CH3:1])[CH:3]=1)[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]参加物
4
実験手順
1 mole of 1-methylimidazole was dissolved in 400 ml of ethanol and 1.2 moles of n-octyl bromide were added. The mixture was then heated to the boiling point for 5 hours. Thereafter, ethanol and excess n-octyl bromide were removed. The residue was purified in ether. In this manner, 250 g of 1-n-octyl-3-methyl-imidazolium bromide were obtained.
後処理
- temperatureThe mixture was then heated to the boiling point for 5 hours
- customThereafter, ethanol and excess n-octyl bromide were removed
- customThe residue was purified in ether
出典と根拠
- ORDレコード
- ord-5d047517faa743fd9d5633632be4f1d5
- 出典データセット
- uspto-grants-1979_04
- 特許番号
- US04150967
反応ノート
読み込み中…