1-Methylimidazole → HCID 178443590、化合物

HRID 26628

反応式

HRID 26628 の反応式
[CH3:1][N:2]1[CH:6]=[CH:5][N:4]=[CH:3]1.[CH2:7]([Br:15])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]>C(O)C>[Br-:15].[CH2:7]([N+:4]1[CH:5]=[CH:6][N:2]([CH3:1])[CH:3]=1)[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]

参加物

4

反応物 2

HCID 13901-MethylimidazoleHCID 81401-Bromooctane

生成物 1

HCID 178443590HCID 178443590、化合物収率 90.8%

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

1 mole of 1-methylimidazole was dissolved in 400 ml of ethanol and 1.2 moles of n-octyl bromide were added. The mixture was then heated to the boiling point for 5 hours. Thereafter, ethanol and excess n-octyl bromide were removed. The residue was purified in ether. In this manner, 250 g of 1-n-octyl-3-methyl-imidazolium bromide were obtained.

後処理

  1. temperatureThe mixture was then heated to the boiling point for 5 hours
  2. customThereafter, ethanol and excess n-octyl bromide were removed
  3. customThe residue was purified in ether

出典と根拠

ORDレコード
ord-5d047517faa743fd9d5633632be4f1d5
出典データセット
uspto-grants-1979_04
特許番号
US04150967

関連ノート

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