Borane → HCID 54510280、化合物
反応式
[NH:1]1[CH2:8][CH2:7][CH2:6][C@H:2]1[C:3]([OH:5])=O.[N+:9]([C:12]1[CH:24]=[C:16]2[C:17](O[C:20](=O)[N:21](C)[C:15]2=[CH:14][CH:13]=1)=O)([O-:11])=[O:10].B>O1CCCC1>[CH3:20][N:21]1[C:15]2[CH:14]=[CH:13][C:12]([N+:9]([O-:11])=[O:10])=[CH:24][C:16]=2[CH2:17][N:1]2[CH2:8][CH2:7][CH2:6][CH:2]2[C:3]1=[O:5]参加物
5
実験手順
This compound is obtained when 1,2,3,11a-tetrahydro- 10-methyl-7-nitro-11H-pyrrolo[2,1-c] [1,4]benzodiazepin-5,11- (10H]-dione (prepared from proline and 5-nitro-N-methylisatoic anhydride by the procedure of Example 1) is treated with 1 M borane in tetrahydrofuran by the procedure of Example 1.
出典と根拠
- ORDレコード
- ord-19c4eaa42ae1422a8786f3ca8fca5a37
- 出典データセット
- uspto-grants-1976_03
- 特許番号
- US03947408
反応ノート
読み込み中…