反応式
[OH-:1].[Na+].[Sn:3]([Cl:7])([Cl:6])([Cl:5])[Cl:4].[Cl-:8].[In+3:9].[Cl-].[Cl-]>O.[N+]([O-])([O-])=O.[Fe+2].[N+]([O-])([O-])=O>[Sn:3]([Cl:7])([Cl:6])([Cl:5])[Cl:4].[Cl-:8].[In+3:9].[Cl-:4].[Cl-:4].[OH-:1]参加物
8
実験手順
Sodium hydroxide (0.75 mol) was dissolved in water (180 ml) to prepare an aqueous alkaline solution. Separately from this alkaline solution, an aqueous solution of tin chloride and indium chloride was prepared by dissolving indium chloride (III) tetrahydrate (0.067 mol) and tin chloride (IV) pentahydrate (0.007 mol) in water (400 ml). To the former aqueous alkaline solution, was added dropwise the latter aqueous solution of tin chloride and indium chloride to form a precipitate of a hydroxide or a hydrate comprising tin and indium. The pH of the precipitate was 10.2. A suspension of the precipitate was aged at room temperature for 20 hours, and then washed with water until the pH of the precipitate reached 7.6.
後処理
- customto prepare an aqueous alkaline solution
出典と根拠
- ORDレコード
- ord-ab1889d9a37a4eda82d1adf42c4ef737
- 出典データセット
- uspto-grants-2008_11
- 特許番号
- US07445858B2
関連ノート
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