Decanoic Acid → Silver(1+) decanoate

HRID 277626

反応式

HRID 277626 の反応式
[C:1]([OH:12])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[OH-].[Na+].C([O-])(=O)CCCCCCCCC.[Na+].[N+]([O-])([O-])=O.[Ag+:32]>O>[C:1]([O-:12])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[Ag+:32]

参加物

6

反応物 4

HCID 2969Decanoic AcidHCID 14798Sodium HydroxideHCID 24470Silver NitrateHCID 4457968Sodium Caprate2 回

生成物 1

HCID 21226017Silver(1+) decanoate

試薬・触媒・溶媒 1

HCID 962Water溶媒2 回

反応条件

温度
60 °C

実験手順

First, silver n-decanoate was prepared by the known procedure. Thus, commercial n-decanoic acid and sodium hydroxide were put in pure water and dissolved under heating at 60° C. to prepare sodium n-decanoate. Separately, an equivalent of silver nitrate was dissolved in pure water and the resulting solution was added to the above aqueous solution of sodium n-decanoate. The silver n-decanoate precipitating out was recovered with a suction filter and dried in a dryer.

後処理

  1. dissolutiondissolved
  2. customThe silver n-decanoate precipitating out was recovered with a suction
  3. filtrationfilter
  4. customdried in a dryer

出典と根拠

ORDレコード
ord-f46b06245fca4c2b804bc12f71303180
出典データセット
uspto-grants-2002_03
特許番号
US06358611B1

関連ノート

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