反応式
[NH2:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][C:10]=2[NH2:12])[CH:5]=[CH:4][CH:3]=1.[F:13][C:14]([F:25])([F:24])[C:15]1[CH:16]=[C:17]([CH:21]=[CH:22][CH:23]=1)[C:18]([Cl:20])=O>>[ClH:20].[F:13][C:14]([F:24])([F:25])[C:15]1[CH:16]=[C:17]([C:18]2[NH:1][C:2]3[CH:3]=[CH:4][CH:5]=[C:6]4[C:11]=3[C:10]([N:12]=2)=[CH:9][CH:8]=[CH:7]4)[CH:21]=[CH:22][CH:23]=1参加物
3
実験手順
1,8-Diaminonaphthalene (15.82 g.; 0.10 mole) and m-trifluoromethylbenzoyl chloride (20.8 g.; 0.10 mole) were reacted in the same procedures as reported in Example 1, yielding 33.3 g. (95.4% yield) of 2-(m-trifluoromethylphenyl)-1H-perimidine hydrochloride, m.p. 280° C. (dec), mass spectrum m/e 312.
後処理
- customyielding 33.3 g
出典と根拠
- ORDレコード
- ord-49d57511993d4538a36b4d6ba6c28f34
- 出典データセット
- uspto-grants-1980_09
- 特許番号
- US04224326
関連ノート
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