Sodium Fluoride → Phenyl Fluoroformate
反応式
[C:1]1([O:7][C:8](Cl)=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[F-:11].[Na+].C1OCCOCCOCCOCCOC1>C(#N)C>[C:1]1([O:7][C:8]([F:11])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1参加物
5
反応条件
- 温度
- 40 °C
実験手順
To a solution of phenylchloroformate in acetonitrile is charged sodium fluoride. To this mixture is charged the 15-crown-5(“15C5”) at ambient temperature. The reaction mixture is then heated to 40° C. for approximately 16 hrs. Reaction completion is monitored by gas chromatography (“G.C.”).
後処理
- customReaction completion
出典と根拠
- ORDレコード
- ord-550de413773c49dd9b5b621e9b040826
- 出典データセット
- uspto-grants-2002_03
- 特許番号
- US06362363B1
反応ノート
読み込み中…