Hydrazine hydrate (1:1) → Arabinosehydrazon

HRID 279931

反応式

HRID 279931 の反応式
[O:1]=[CH:2][C@H:3]([C@@H:5]([C@@H:7]([CH2:9]O)[OH:8])[OH:6])[OH:4].O.[NH2:12][NH2:13]>CO>[CH:9](=[N:12][NH2:13])[C@H:7]([C@@H:5]([C@@H:3]([CH2:2][OH:1])[OH:4])[OH:6])[OH:8]

参加物

4

反応物 2

HCID 24654Hydrazine hydrate (1:1)HCID 66308D-Arabinose

生成物 1

HCID 86740783Arabinosehydrazon

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

A solution of 4.0 g of D-arabinose in 10 ml of methanol and 10 ml of hydrazine hydrate was stirred overnight, then evaporated to dryness in vacuo. The residue was triturated with 25 ml of methanol and the solid was collected, giving 3.5 g of D-arabinose hydrazone.

後処理

  1. customevaporated to dryness in vacuo
  2. customThe residue was triturated with 25 ml of methanol
  3. customthe solid was collected

出典と根拠

ORDレコード
ord-ebf88657c39e4ad8abc375b13788fe63
出典データセット
uspto-grants-1986_05
特許番号
US04587331

関連ノート

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