Oxalyl chloride → 2,3-Dichloro-6-iodobenzoic acid chloride
反応式
[Cl:1][C:2]1[C:10]([Cl:11])=[CH:9][CH:8]=[C:7]([I:12])[C:3]=1[C:4](O)=[O:5].C(Cl)(=O)C([Cl:16])=O>CN(C=O)C.C(OCC)(=O)C>[Cl:1][C:2]1[C:10]([Cl:11])=[CH:9][CH:8]=[C:7]([I:12])[C:3]=1[C:4]([Cl:16])=[O:5]参加物
5
実験手順
DMF (one drop) was added to a stirred solution of 2,3-dichloro-6-iodobenzoic acid (1.53 g, 4.83 mmol) and oxalyl chloride (2 ml) in ethyl acetate (20 ml). After 2 hours, the solution was evaporated and the product was used immediately.
後処理
- customthe solution was evaporated
出典と根拠
- ORDレコード
- ord-7726a461dd284d93b0a1fcdd654e9b25
- 出典データセット
- uspto-grants-2001_04
- 特許番号
- US06211189B1
反応ノート
読み込み中…