Aniline → Benzeneethanamine, N-phenyl-

HRID 325137

反応式

HRID 325137 の反応式
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:8]=[CH:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>C(OCC)(=O)C.CCCCCC>[C:10]1([CH2:9][CH2:8][NH:1][C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

参加物

4

反応物 2

HCID 6115AnilineHCID 7501Styrene

生成物 1

HCID 74443Benzeneethanamine, N-phenyl-収率 78%

試薬・触媒・溶媒 1

HCID 21226206Ethyl acetate hexane溶媒

実験手順

According to GWM, 0.011 mol (=1.00 ml) of aniline and 0.011 mol (=1.25 ml) of styrene are reacted with one another. The product is isolated by column chromatography using ethyl acetate/n-hexane (1:3) as eluent, the product N-phenylethylaniline being obtained as a yellow liquid.

後処理

  1. customare reacted with one another
  2. customThe product is isolated by column chromatography

出典と根拠

ORDレコード
ord-cde6fc26c17d47a3be4c2061a84b856f
出典データセット
uspto-grants-2001_04
特許番号
US06222073B1

関連ノート

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