Triethylaluminum → Triethylaluminum

HRID 325750ノート

反応式

HRID 325750 の反応式
[CH2:1]([Mg:5][CH2:6][CH2:7]CC)[CH2:2][CH2:3][CH3:4].[CH2:10]([Al:12]([CH2:15][CH3:16])[CH2:13][CH3:14])[CH3:11]>CCCCCCC>[CH2:1]([Mg:5][CH2:6][CH3:7])[CH2:2][CH2:3][CH3:4].[CH2:10]([Al:12]([CH2:15][CH3:16])[CH2:13][CH3:14])[CH3:11]

参加物

5

反応物 2

HCID 16682930TriethylaluminumHCID 178448196HCID 178448196、化合物

生成物 2

HCID 16682930TriethylaluminumHCID 178448194HCID 178448194、化合物

試薬・触媒・溶媒 1

HCID 8900Heptane溶媒2 回

実験手順

In this case, the n-heptane solution of the complex consisting of di-n-butyl magnesium and tri-ethyl aluminum which was used in Example 51 was replaced with a reaction product obtained from 161 ml of an n-heptane solution of n-butyl ethyl magnesium (manufactured by Texas Alkyls Inc. of U.S.A., MAGALABEM, Mg concentration 0.65 mol/liter) and 4.3 ml of tri-ethyl aluminum. With the exception of this, a catalytic component was prepared and propylene was polymerized in exactly the same manner as in Example 1. The results of polymerization were: A=445, H.I.=94.8 and ρB=0.45.

出典と根拠

ORDレコード
ord-58b702f309ce4da4bad67aed9f544bc8
出典データセット
uspto-grants-1984_04
特許番号
US04442225

反応ノート

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