Sodium Hydroxide → Sodium 6-methoxynicotinate

HRID 339380

反応式

HRID 339380 の反応式
[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:6]([C:7]([O:9]C)=[O:8])=[CH:5][N:4]=1.[OH-].[Na+:14]>O1CCOCC1>[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:6]([C:7]([O-:9])=[O:8])=[CH:5][N:4]=1.[Na+:14]

参加物

4

反応物 2

HCID 14798Sodium HydroxideHCID 586039Methyl 6-methoxypyridine-3-carboxylate

生成物 1

HCID 23717611Sodium 6-methoxynicotinate

試薬・触媒・溶媒 1

HCID 312751,4-Dioxane溶媒

実験手順

methyl 6-methoxynicotinate (2.097 g, 12.56 mmol) was dissolved in dioxane (30 mL). An aqueous solution of NaOH (1.0N, 25 mL) was added to the solution and the mixture was stirred at room temperature overnight. The solvent was removed under reduced pressure to provide 2.2 g of sodium 6-methoxynicotinate.

後処理

  1. customThe solvent was removed under reduced pressure

出典と根拠

ORDレコード
ord-0482b300a3214a2a9e2d4a88299a8574
出典データセット
uspto-grants-2014_11
特許番号
US08895050B2

関連ノート

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