反応式
C([N:4]1[C:12]2[C:7](=[CH:8][C:9]([O:28][CH3:29])=[C:10]([N:13]3[CH2:18][C@H:17]([CH3:19])[N:16](CC4C=CC=CC=4)[C@H:15]([CH3:27])[CH2:14]3)[CH:11]=2)[CH2:6][CH2:5]1)(=O)C>Cl.[Pd]>[CH3:27][C@H:15]1[NH:16][C@@H:17]([CH3:19])[CH2:18][N:13]([C:10]2[CH:11]=[C:12]3[C:7]([CH2:6][CH2:5][NH:4]3)=[CH:8][C:9]=2[O:28][CH3:29])[CH2:14]1参加物
4
実験手順
The title compound was prepared from D4 by hydrogenation over 10% Pd/C using a similar procedure to Example 45 (98%), followed by hydrolysis in 2M HCl using a similar procedure to Description 3 (80%) to afford the product as a pale brown solid
出典と根拠
- ORDレコード
- ord-7364dfedd8244a10939e58d2c4a3bb0e
- 出典データセット
- uspto-grants-2004_06
- 特許番号
- US06747030B1
関連ノート
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