Allylamine → 2,2'-Azobis[n-(2-propenyl)-2-methylpropionamide]

HRID 359575

反応式

HRID 359575 の反応式
[N:1]([C:10]([CH3:16])([CH3:15])[C:11]([O:13]C)=O)=[N:2][C:3]([CH3:9])([CH3:8])[C:4]([O:6]C)=O.[CH2:17]([NH2:20])[CH:18]=[CH2:19]>CO>[N:2]([C:3]([CH3:8])([CH3:9])[C:4]([NH:20][CH2:17][CH:18]=[CH2:19])=[O:6])=[N:1][C:10]([CH3:16])([CH3:15])[C:11]([NH:20][CH2:17][CH:18]=[CH2:19])=[O:13]

参加物

4

反応物 2

HCID 7853AllylamineHCID 757631,1'-Dimethyl 2,2'-(1,2-diazenediyl)bis(2-methylpropanoate)

生成物 1

HCID 157247352,2'-Azobis[n-(2-propenyl)-2-methylpropionamide]

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

Dimethyl 2,2'-azobis(2-methylpropionate) in an amount of 41.9 g, 48 ml of methanol, and 43 g of a 28% CH3ONa methanol solution were mixed and stirred for dissolution, followed by dropwise addition of 25 g of allylamine to react at 19° to 21° C. for 20 hours.

後処理

  1. customto react at 19° to 21° C. for 20 hours

出典と根拠

ORDレコード
ord-cbc849f2079f4b2e89bfcd0e603da8a8
出典データセット
uspto-grants-1991_03
特許番号
US05001228

関連ノート

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