Allylamine → 2,2'-Azobis[n-(2-propenyl)-2-methylpropionamide]
反応式
[N:1]([C:10]([CH3:16])([CH3:15])[C:11]([O:13]C)=O)=[N:2][C:3]([CH3:9])([CH3:8])[C:4]([O:6]C)=O.[CH2:17]([NH2:20])[CH:18]=[CH2:19]>CO>[N:2]([C:3]([CH3:8])([CH3:9])[C:4]([NH:20][CH2:17][CH:18]=[CH2:19])=[O:6])=[N:1][C:10]([CH3:16])([CH3:15])[C:11]([NH:20][CH2:17][CH:18]=[CH2:19])=[O:13]参加物
4
実験手順
Dimethyl 2,2'-azobis(2-methylpropionate) in an amount of 41.9 g, 48 ml of methanol, and 43 g of a 28% CH3ONa methanol solution were mixed and stirred for dissolution, followed by dropwise addition of 25 g of allylamine to react at 19° to 21° C. for 20 hours.
後処理
- customto react at 19° to 21° C. for 20 hours
出典と根拠
- ORDレコード
- ord-cbc849f2079f4b2e89bfcd0e603da8a8
- 出典データセット
- uspto-grants-1991_03
- 特許番号
- US05001228
反応ノート
読み込み中…