Butylamine → HCID 178449232、化合物

HRID 372223

反応式

HRID 372223 の反応式
CS/[C:3](/[NH2:6])=[N:4]/[NH2:5].[IH:7].[NH2:8][CH2:9][CH2:10][CH2:11][CH3:12]>O>[IH:7].[NH2:5][NH:4][C:3]([NH:8][CH2:9][CH2:10][CH2:11][CH3:12])=[NH:6]

参加物

4

反応物 2

HCID 8007ButylamineHCID 6508896Methyl hydrazinecarbimidothioate hydroiodide

生成物 1

HCID 178449232HCID 178449232、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

S-Methylisothiosemicarbazide hydroiodide (46.6 g) and 1-aminobutane (48 ml) and water (100 ml) were heated under reflux for 1 hour. The resulting solution was evaporated to an oil which was crystallised from amyl alcohol/80-100 PE, to give the title compound (a).

後処理

  1. temperatureunder reflux for 1 hour
  2. customThe resulting solution was evaporated to an oil which
  3. customwas crystallised from amyl alcohol/80-100 PE

出典と根拠

ORDレコード
ord-f2bacff0b3604575b7f45e3420a48d67
出典データセット
uspto-grants-1978_05
特許番号
US04089962

関連ノート

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