Hydroquinone → Dicumyl peroxide

HRID 380062ノート

反応式

HRID 380062 の反応式
C[O-].[Na+].[O-2].[Al+3].[O-2].[O-2].[Al+3].[C:9]1([CH:16]=[CH:15][C:13](O)=[CH:12][CH:11]=1)O.C[CH2:18][C:19]([O:23][O:24][C:25](OO)([CH2:27]C)[CH3:26])(OO)[CH3:20].CN(C)[C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1>ClCCl.C1(C)C=CC=CC=1>[C:19]([O:23][O:24][C:25]([C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1)([CH3:27])[CH3:26])([C:9]1[CH:16]=[CH:15][CH:13]=[CH:12][CH:11]=1)([CH3:20])[CH3:18]

参加物

8

反応物 5

HCID 785HydroquinoneHCID 949N,N-DimethylanilineHCID 3672772Methyl ethyl ketone peroxideHCID 9989226AluminaHCID 10942334Sodium Methoxide

生成物 1

HCID 6641Dicumyl peroxide

試薬・触媒・溶媒 2

HCID 1140Toluene溶媒HCID 6344Dichloromethane溶媒

実験手順

Sodium methoxide (NaOCH3), toluene (anhydrous), dichloromethane, hexanes, activated neutral aluminum oxide (60 to 50 mesh), hydroquinone, methyl ethyl ketone peroxide, dimethylaniline, dicumylperoxide were obtained from commercial sources and used as received.

出典と根拠

ORDレコード
ord-d901dd241c564dd493adae2c78ed4c08
出典データセット
uspto-grants-2001_10
特許番号
US06300457B1

反応ノート

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