Ammonia → Nickel cobalt aluminum hydroxide

HRID 381258

反応式

HRID 381258 の反応式
[N+]([O-])([O-])=[O:2].[Ni+2:5].[N+]([O-])([O-])=[O:7].[N+]([O-])([O-])=[O:11].[Co+2:14].[N+]([O-])([O-])=[O:16].[N+]([O-])([O-])=O.[Al+3:23].[N+]([O-])([O-])=O.[N+]([O-])([O-])=O.N.[OH-:33].[Na+]>>[OH-:2].[Al+3:23].[Co+2:14].[Ni+2:5].[OH-:7].[OH-:11].[OH-:16].[OH-:33].[OH-:2].[OH-:2]

参加物

6

実験手順

In this way, the reaction was conducted for 48 hours while continuously adding the aqueous solution of mixture of nickel nitrate, cobalt nitrate and aluminum nitrate, the aqueous ammonia and the aqueous solution of sodium hydroxide to the reactor. During the reaction, the concentration of ammonia in the reaction mixture (slurry) in the reactor was kept within a range from 1.0 to 1.3 mol/L and the reaction temperature was kept at 30° C.±1° C. with a temperature controller, After the completion of the reaction, the slurry in the reactor was filtered, washed with water and dried to provide a powder of nickel cobalt aluminum hydroxide.

後処理

  1. additionwhile continuously adding
  2. customDuring the reaction
  3. customwas kept at 30° C.±1° C. with a temperature controller
  4. customAfter the completion of the reaction
  5. filtrationthe slurry in the reactor was filtered
  6. washwashed with water
  7. customdried

出典と根拠

ORDレコード
ord-a1ba84fa1163457ea5d7b01e9bd8235e
出典データセット
uspto-grants-2001_10
特許番号
US06306787B1

関連ノート

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