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Isopropylamine → 5-(n-Isopropylcarbamoyl)-2-[1-(3-nitro-2-pyridyl)piperazin-4-yl-carbonyl]pyridine

HRID 381365
ノート
印刷プレビュー

反応式

HRID 381365 の反応式
[N+:1]([C:4]1[C:5]([N:10]2[CH2:15][CH2:14][N:13]([C:16]([C:18]3[CH:26]=[CH:25][C:21]([C:22]([OH:24])=O)=[CH:20][N:19]=3)=[O:17])[CH2:12][CH2:11]2)=[N:6][CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].C(Cl)(=O)C(C)(C)C.[CH:34]([N:37](CC)C(C)C)([CH3:36])[CH3:35].C(N)(C)C>C(Cl)Cl.C(N(CC)CC)C>[CH:34]([NH:37][C:22]([C:21]1[CH:25]=[CH:26][C:18]([C:16]([N:13]2[CH2:12][CH2:11][N:10]([C:5]3[C:4]([N+:1]([O-:3])=[O:2])=[CH:9][CH:8]=[CH:7][N:6]=3)[CH2:15][CH2:14]2)=[O:17])=[N:19][CH:20]=1)=[O:24])([CH3:36])[CH3:35]
参加物実験手順後処理出典と根拠反応ノート

参加物

7

反応物 4

HCID 6363IsopropylamineHCID 62493Pivaloyl chlorideHCID 81531DiisopropylethylamineHCID 183628396-[1-(3-Nitro-2-pyridyl)piperazin-4-yl-carbonyl]nicotinic acid

生成物 1

HCID 183628135-(n-Isopropylcarbamoyl)-2-[1-(3-nitro-2-pyridyl)piperazin-4-yl-carbonyl]pyridine収率 78%

試薬・触媒・溶媒 2

HCID 6344
Dichloromethane
溶媒
HCID 8471Triethylamine溶媒

実験手順

Triethylamine (0.85 ml) was added to 6-[1-(3-nitro-2-pyridyl)piperazin-4-yl-carbonyl]nicotinic acid (2 g) in methylene chloride (25 ml) for dissolution and cooled. With the slow addition of pivaloyl chloride (0.7 ml) at 0° C.˜5° C., the mixture was stirred at 5° C.˜10° C. for 2 hours. With the addition of N,N-diisopropylethylamine (1.1 ml) and isopropylamine (0.55 ml), the mixture was stirred at 10° C.˜15° C. for 3 hours. The reaction mixture was washed with an aqueous sodium bicarbonate and water twice. The separated organic layer was dried over magnesium sulfate and concentrated under reduced pressure. The residue was dissolved in chloroform (15 ml) and with the slow addition of ether, crystals were precipitated. For 2-hours stirring, the precipitate was filtered, washed (ether) and dried to give a desired compound of 1.74 g (yield: 78%).

後処理

  1. temperaturecooled
  2. stirringthe mixture was stirred at 10° C.˜15° C. for 3 hours
  3. washThe reaction mixture was washed with an aqueous sodium bicarbonate and water twice
  4. dry with materialThe separated organic layer was dried over magnesium sulfate
  5. concentrationconcentrated under reduced pressure
  6. dissolutionThe residue was dissolved in chloroform (15 ml) and with the slow addition of ether, crystals
  7. customwere precipitated
  8. stirringFor 2-hours stirring
  9. filtrationthe precipitate was filtered
  10. washwashed (ether)
  11. customdried

出典と根拠

ORDレコード
ord-cb25f6fce5564821a8203a3b17e8b609
出典データセット
uspto-grants-2001_10
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US06306860B1

反応ノート

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