Dimethyl Sulfide → Trimethylsulfonium Triflate
反応式
[CH3:1][S:2][CH3:3].[CH3:4][O:5][S:6]([C:9]([F:12])([F:11])[F:10])(=[O:8])=[O:7]>ClCCl>[O-:8][S:6]([C:9]([F:12])([F:11])[F:10])(=[O:7])=[O:5].[CH3:1][S+:2]([CH3:4])[CH3:3]参加物
4
実験手順
16 mmol of dimethyl sulfide was dissolved in 10 ml of dichloromethane at 0° C., and about 17 mmol of methyltrifluoromethane sulfonate was slowly dripped to the mixture to obtain a white solid product. The solid product was filtered and dried for 1 hour in an oven at 50° C. to obtain the following product:
後処理
- customto obtain a white solid product
- filtrationThe solid product was filtered
- customdried for 1 hour in an oven at 50° C.
- customto obtain the following product
出典と根拠
- ORDレコード
- ord-5cc9413dfef7447db1b13d03a866a5a8
- 出典データセット
- uspto-grants-2013_09
- 特許番号
- US08536347B2
反応ノート
読み込み中…