2,3-Dihydroxybutanedioic Acid → Dilithium tartrate
反応式
[C:1]([OH:10])(=[O:9])[CH:2]([CH:4]([C:6]([OH:8])=[O:7])[OH:5])[OH:3].[OH-].[Li+:12]>O>[C:1]([O-:10])(=[O:9])[CH:2]([CH:4]([C:6]([O-:8])=[O:7])[OH:5])[OH:3].[Li+:12].[Li+:12]参加物
4
実験手順
Tartaric acid (15.0 g, 0.1 mole) is dissolved in 40 ml. water and treated with lithium hydroxide (8.4 g, 0.2 mole). The resulting solution is evaporated to a small volume under reduced pressure and the residue is treated with p-dioxane. The resulting precipitate is filtered and dried under vacuum to give the di-lithium tartarate (17.7 g).
後処理
- customThe resulting solution is evaporated to a small volume under reduced pressure
- additionthe residue is treated with p-dioxane
- filtrationThe resulting precipitate is filtered
- customdried under vacuum
出典と根拠
- ORDレコード
- ord-8d6a27a52a8346bb9c5cc59e0c5b2a6a
- 出典データセット
- uspto-grants-1981_04
- 特許番号
- US04260627
反応ノート
読み込み中…