ホームMCPワークベンチSkills
ホームワークベンチ通知マイページ
llms.txt · MCPガイドプライバシーポリシー · 利用規約 · サポートv1.8.0
  1. ホーム
  2. /反応

Hydrochloric Acid → HCID 86761916、化合物

HRID 446582
ノート
印刷プレビュー

反応式

HRID 446582 の反応式
[NH2:1][C:2]([NH:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]([O:12]C)=O)=[S:3].[OH-].[Na+].Cl.[C:17]1([C:37]2[CH:42]=[CH:41][CH:40]=[CH:39][CH:38]=2)[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=1[NH:23][C:24](=[O:36])[O:25][CH:26]1[CH2:31][CH2:30][N:29]([CH2:32][CH2:33][NH:34][CH3:35])[CH2:28][CH2:27]1.Cl.C(N=C=NCCCN(C)C)C.C(N(CC)CC)C.C(=O)([O-])O.[Na+]>CO>[C:17]1([C:37]2[CH:42]=[CH:41][CH:40]=[CH:39][CH:38]=2)[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=1[NH:23][C:24](=[O:36])[O:25][CH:26]1[CH2:31][CH2:30][N:29]([CH2:32][CH2:33][N:34]([C:10](=[O:12])[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][NH:4][C:2]([NH2:1])=[S:3])[CH3:35])[CH2:28][CH2:27]1
参加物実験手順後処理出典と根拠反応ノート

参加物

9

反応物 7

HCID 313Hydrochloric AcidHCID 8471TriethylamineHCID 14798Sodium HydroxideHCID 516892Sodium BicarbonateHCID 27239391,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochlorideHCID 4962408methyl 6-[(aminocarbonothioyl)amino]hexanoate
HCID 56643603
1-(2-(Methylamino)ethyl)piperidin-4-yl [1,1'-biphenyl]-2-ylcarbamate

生成物 1

HCID 86761916HCID 86761916、化合物収率 34%

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

Methyl 6-[(aminocarbonothioyl)amino]hexanoate (335 mg, 1.64 mmol) was dissolved in methanol (10 mL), a 1 N aqueous sodium hydroxide solution (2.46 mL, 2.46 mmol) was added, and the mixture was stirred at room temperature for 4 hours. After the reaction was completed, 1 N hydrochloric acid (2.46 mL, 2.46 mmol) was added, and then the solvent was evaporated under reduced pressure. The resulting residue was dissolved in dichloromethane, 1-[2-(methylamino)ethyl]piperidin-4-yl biphenyl-2-ylcarbamate (578 mg, 1.64 mmol), 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride (469 mg, 2.46 mmol) and triethylamine (0.342 mL, 2.46 mmol) were added, and the mixture was stirred overnight at room temperature. After the reaction was completed, a saturated aqueous sodium hydrogencarbonate solution was added, the mixture was extracted 3 times with methylene chloride, and the resulting organic layer was dried with anhydrous sodium sulfate. The solvent was evaporated under reduced pressure, and the resulting residue was purified by NH silica gel column chromatography (elution solvents, n-hexane:ethyl acetate:methanol=1:1:0→0:10:0→0:9:1, v/v/v) to give the title compound (291 mg; yield, 34%).

後処理

  1. customthe solvent was evaporated under reduced pressure
  2. dissolutionThe resulting residue was dissolved in dichloromethane
  3. stirringthe mixture was stirred overnight at room temperature
  4. extractionthe mixture was extracted 3 times with methylene chloride
  5. dry with materialthe resulting organic layer was dried with anhydrous sodium sulfate
  6. customThe solvent was evaporated under reduced pressure
  7. customthe resulting residue was purified by NH silica gel column chromatography (elution solvents, n-hexane:ethyl acetate:methanol=1:1:0→0:10:0→0:9:1, v/v/v)

出典と根拠

ORDレコード
ord-9bd726d10d004918996dad66a65b89d3
出典データセット
uspto-grants-2013_07
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US08476253B2

反応ノート

読み込み中…

このページの内容参加物実験手順後処理出典と根拠反応ノート