Aminoacetaldehyde dimethyl acetal → 7-Bromo-6-methylisoquinoline
反応式
[Br:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][C:9]=1[CH3:10])[CH:5]=O.CO[CH:13](OC)[CH2:14][NH2:15]>>[Br:1][C:2]1[CH:3]=[C:4]2[C:7]([CH:13]=[CH:14][N:15]=[CH:5]2)=[CH:8][C:9]=1[CH3:10]参加物
3
実験手順
This compound was prepared by using procedures analogous to those described for the synthesis of Example 75, Step 1 starting from 3-bromo-4-methylbenzaldehyde (Aldrich, Cat. #4017458) and. aminoacetaldehyde dimethyl acetal. Analytic LCMS (M+H)+: m/z=221.95/223.95.
後処理
- customThis compound was prepared
出典と根拠
- ORDレコード
- ord-66fcfe8a5a6d463f9b6baa757d41bd3f
- 出典データセット
- uspto-grants-2013_07
- 特許番号
- US08481732B2
反応ノート
読み込み中…