反応式
[N+:1]([C:4]1[CH:9]=[C:8]([C:10]([F:13])([F:12])[F:11])[CH:7]=[CH:6][C:5]=1[CH2:14][C:15]([O:17]C)=O)([O-])=O>[Pd]>[F:11][C:10]([F:13])([F:12])[C:8]1[CH:9]=[C:4]2[C:5]([CH2:14][C:15](=[O:17])[NH:1]2)=[CH:6][CH:7]=1参加物
3
反応条件
- 温度
- 100 °C
実験手順
Methyl 2-nitro-4-trifluoromethylphenylacetate (26 mg) was hydrogenated over 10% palladium on carbon and then heated at 100° C. for 3 hours. The catalyst was removed by filtration and the solvent evaporated to give the title compound.
後処理
- customThe catalyst was removed by filtration
- customthe solvent evaporated
出典と根拠
- ORDレコード
- ord-8297bf6395c54394842ec4283eb5610d
- 出典データセット
- uspto-grants-2007_03
- 特許番号
- US07189721B2
関連ノート
読み込み中…