Chloride → N,N-Dimethyl-N-(prop-2-en-1-yl)hexadecan-1-aminium chloride

HRID 461606

反応式

HRID 461606 の反応式
[CH2:1]([Cl:4])[CH:2]=[CH2:3].[CH3:5][N:6]([CH3:23])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[Cl-]>>[Cl-:4].[CH2:1]([N+:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])([CH3:5])[CH3:23])[CH:2]=[CH2:3]

参加物

4

反応物 3

HCID 312ChlorideHCID 7850Allyl chlorideHCID 16221Dimethylhexadecylamine

生成物 1

HCID 20503036N,N-Dimethyl-N-(prop-2-en-1-yl)hexadecan-1-aminium chloride

実験手順

Allyl hexadecyl dimethyl ammonium chloride was prepared by reacting allyl chloride and dimethyl hexadecyl amine as set forth in Example 1. 17.8 grams of the chloride in 23.5% aqueous solution were treated with a stoichiometric excess of AgF in aqueous solution until analysis of the filtrate showed only a trace of chloride ion present. Excess silver ion was removed by the careful addition of NaCl, AgCl being removed by filtration.

後処理

  1. customExcess silver ion was removed by the careful addition of NaCl, AgCl being
  2. customremoved by filtration

出典と根拠

ORDレコード
ord-c85224a51c4c451ebd14d9ed4e23eca9
出典データセット
uspto-grants-1977_12
特許番号
US04064091

関連ノート

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