Isopropylamine → 2-chloroethanephosphonic acid isopropyl ester N-monoisopropylamide

HRID 462009

反応式

HRID 462009 の反応式
[Cl-].[CH:2]([NH:5][P:6]([CH2:9][CH2:10][Cl:11])(=[O:8])[OH:7])([CH3:4])[CH3:3].ClCCP(Cl)(Cl)=[O:16].[CH:19](N)([CH3:21])[CH3:20]>C1(C)C=CC=CC=1>[CH:2]([NH-:5])([CH3:4])[CH3:3].[CH:19]([O:16][P:6]([CH2:9][CH2:10][Cl:11])(=[O:8])[OH:7])([CH3:21])[CH3:20]

参加物

5

反応物 3

HCID 6363IsopropylamineHCID 69645(2-Chloroethyl)phosphonic dichlorideHCID 867353082-chloroethanephosphonic acid N-monoisopropylamide chloride

生成物 1

HCID 867353092-chloroethanephosphonic acid isopropyl ester N-monoisopropylamide

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

The 2-chloroethane-phosphonic acid N-mono-isopropylamide chloride used as starting product was prepared from 2-chloroethane-phosphonic acid dichloride and iso-propylamine in toluene at 0° C. Yield: 91% of the theory, nD28 = 1.4854.

出典と根拠

ORDレコード
ord-6d8821fac516425287dcfb50e1433db5
出典データセット
uspto-grants-1977_12
特許番号
US04065288

関連ノート

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