反応式
[F:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([F:11])[CH:10]=1)[C:5](O)=[O:6].S(Cl)([Cl:14])=O>>[F:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([F:11])[CH:10]=1)[C:5]([Cl:14])=[O:6]参加物
3
実験手順
1.63 g (10.00 mmol) 3,5-difluoro-benzoic acid were mixed with 20 mL thionyl chloride and boiled for 2 h. The reaction mixture was evaporated to dryness and coevaporated twice with toluene. The residue was reacted further as the crude product.
後処理
- customThe reaction mixture was evaporated to dryness
- customThe residue was reacted further as the crude product
出典と根拠
- ORDレコード
- ord-a565cd0d833a42f3b36e645c6b592ea7
- 出典データセット
- uspto-grants-2014_01
- 特許番号
- US08629137B2
関連ノート
読み込み中…