反応式
[C:1]([O:10]CC(CO)O)(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[CH2:16]([C:18]([CH2:22][OH:23])([CH2:20][OH:21])[CH3:19])[OH:17].C(OC)(=O)C1C(=CC=CC=1)O.C[O-].[Na+]>>[C:1]([OH:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[CH2:16]([C:18]([CH2:22][OH:23])([CH2:20][OH:21])[CH3:19])[OH:17]参加物
5
実験手順
Trimethylolethane salicylate was prepared by the method described in Example 1 for the preparation of glycerol salicylate except that the reactants were trimethylolethane (60.1 g; 0.5 moles), methyl salicylate (119.7 g; 0.788 moles), sodium methoxide (0.82 g; 0.015 moles). The final methyl salicylate level was 10.0%.
出典と根拠
- ORDレコード
- ord-7cf1c8d830fe483db8fd085ee7f9672d
- 出典データセット
- uspto-grants-1989_12
- 特許番号
- US04886843
関連ノート
読み込み中…