Ethyl chloroformate → HCID 85773191、化合物

HRID 477749

反応式

HRID 477749 の反応式
[C:1]1([NH:7][NH:8][C:9]([NH2:11])=[S:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl[C:13]([O:15][CH2:16][CH3:17])=[O:14]>C(O)C>[CH2:16]([O:15][C:13]([N:7]([C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1)[NH:8][C:9]([NH2:11])=[S:10])=[O:14])[CH3:17]

参加物

4

反応物 2

HCID 10928Ethyl chloroformateHCID 27810941-Phenylthiosemicarbazide

生成物 1

HCID 85773191HCID 85773191、化合物

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

A mixture of 1-phenylthiosemicarbazide (25 g), ethanol (180 ml) and ethyl chloroformate (17 ml) was heated under reflux with stirring for 30 minutes. The mixture was cooled to room temperature and the solid was filtered, washed with ethanol and then with ether to give 28.9 g of the desired product.

後処理

  1. temperaturewas heated
  2. temperatureunder reflux
  3. filtrationthe solid was filtered
  4. washwashed with ethanol

出典と根拠

ORDレコード
ord-ec16df487b4344ac9ab14b8560048c96
出典データセット
uspto-grants-1989_12
特許番号
US04889553

関連ノート

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