Azobisisobutyronitrile → HCID 86759231、化合物
反応式
[C:1]12([C:11]3([C:21]([O-:23])=[O:22])[CH2:16][CH:15]4[CH2:17][C:12]3([CH:18]([CH3:20])[CH3:19])[CH:13]=[CH:14]4)[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.[C:24]1(=[O:30])[O:29][C:27](=[O:28])[CH:26]=[CH:25]1.CC(N=NC(C#N)(C)C)(C#N)C>C1COCC1>[C:1]12([C:11]3([C:21]([O-:23])=[O:22])[CH2:16][CH:15]4[CH2:17][C:12]3([CH:18]([CH3:20])[CH3:19])[CH:13]=[CH:14]4)[CH2:2][CH:3]3[CH2:9][CH:7]([CH2:6][CH:5]([CH2:4]3)[CH2:10]1)[CH2:8]2.[C:27]1(=[O:28])[O:29][C:24](=[O:30])[CH:25]=[CH:26]1参加物
5
実験手順
10.8 g of 1-adamantyl-1-methylethyl-5-norbornene-2-carboxylate prepared in Example 1, and 3.37 g of maleic anhydride were dissolved in 7.1 9 of THF. 0.112 g of AIBN was added to the resultant, degassed and polymerized at a temperature of about 65° C. for about 24 hours.