反応式
[F-:1].[K+].[F:3][C:4]([F:12])([C:8]([F:11])([F:10])[F:9])[C:5](F)=[O:6]>C(#N)C>[F:1][C:4]([F:12])([F:3])[C:5]([C:8]([F:11])([F:10])[F:9])([OH:6])[C:4]([F:12])([F:3])[C:8]([F:11])([F:10])[F:9]参加物
4
反応条件
- 温度
- -196 °C
実験手順
By operating as in the above examples, 0.26 g of KF (4.5 mmol) was charged to the reactor, and then 4.0 ml of anhydrous acetonitrile was injected through the pierceable cap; the whole was then cooled down to -196° C. with the residual air being evacuated; then, 2.0 mmol of pentafluoropropionyl fluoride
後処理
- additionwas charged to the reactor
- custombeing evacuated
出典と根拠
- ORDレコード
- ord-26b6efaca80344a497d3f837a6d8c214
- 出典データセット
- uspto-grants-1993_07
- 特許番号
- US05227539
関連ノート
読み込み中…