反応式
[CH2:1]([Mg]Cl)[C:2]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)([CH3:4])[CH3:3].C(Cl)C(C1C=CC=CC=1)(C)C.[Mg].[CH3:25][Si:26](Cl)([Cl:28])[Cl:27]>C1COCC1>[CH2:1]([CH2:25][SiH:26]([Cl:28])[Cl:27])[C:2]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)([CH3:4])[CH3:3]参加物
6
実験手順
In accord with the procedure of Example 1, neophylmagnesium chloride was prepared from 674 g (4 mol) of neophyl chloride and 105 g (4.4 mol) of magnesium turnings in 1.5 liters of dry THF. The neophylmagnesium chloride was added to 598 g (4 mol) of methyltrichlorosilane and 2 g of cuprous cyanide in 500 ml of THF. 640 g (65% of theory) of neophylmethyldichlorosilane was obtained.
出典と根拠
- ORDレコード
- ord-c8ea5e0ccad847beb6efceb6b6122ccd
- 出典データセット
- uspto-grants-1994_03
- 特許番号
- US05296624
関連ノート
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