反応式
[OH:1][C:2]1[CH:20]=[CH:19][C:5]([O:6][C:7]2[CH:18]=[CH:17][C:10]([CH2:11][NH:12][C:13](=[O:16])[CH2:14][CH3:15])=[CH:9][CH:8]=2)=[CH:4][CH:3]=1.Br[C:22]1([CH2:31][CH2:32][O:33][CH2:34][CH3:35])[C:27](=[O:28])[NH:26][C:25](=[O:29])[NH:24][C:23]1=[O:30].CCCCC=CCCCC.C1(F)(C2(F)OC(C(F)(F)F)(C(F)(F)F)OC2(F)F)OC(C(F)(F)F)(C(F)(F)F)OC1(F)F.C(N)(=O)CC>C(#N)C>[CH2:34]([O:33][CH2:32][CH2:31][C:22]1([O:1][C:2]2[CH:3]=[CH:4][C:5]([O:6][C:7]3[CH:18]=[CH:17][C:10]([CH2:11][NH:12][C:13](=[O:16])[CH2:14][CH3:15])=[CH:9][CH:8]=3)=[CH:19][CH:20]=2)[C:23](=[O:30])[NH:24][C:25](=[O:29])[NH:26][C:27]1=[O:28])[CH3:35]参加物
7
反応物 5
生成物 1
試薬・触媒・溶媒 1
実験手順
Following the procedure outlined for the preparation of Example 1, N-[4-(4-hydroxy-phenoxy)-benzyl]-propionamide (0.13 g, 0.47 mmol) was reacted with 5-bromo-5-(2-ethoxy-ethyl)-pyrimidine-2,4,6-trione (0.13 g, 0.48 mmol), 1,5,7-trazabicyclo[4.4.0]dec-5-ene bound to polystyrene crosslinked with 2% DVB (PTBD, Fluka, 0.31 g) and 1.55 mL of acetonitrile, benzyl)-propionamide (0.060 g) as a colorless solid.
出典と根拠
- ORDレコード
- ord-4a89fc67434542439b5e46a12ded1604
- 出典データセット
- uspto-grants-2004_03
- 特許番号
- US06706723B2
関連ノート
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