Hydrochloric Acid → Sodium Dilysine Succinate Hydrochloride

HRID 53072

反応式

HRID 53072 の反応式
O.[NH2:2][C@H:3]([C:9]([OH:11])=[O:10])[CH2:4][CH2:5][CH2:6][CH2:7][NH2:8].[C:12]([O-:19])(=[O:18])[CH2:13][CH2:14][C:15]([O-:17])=[O:16].[Na+:20].[Na+].C(O)(=O)CCC(O)=O.[ClH:30]>O>[ClH:30].[C:12]([O-:19])(=[O:18])[CH2:13][CH2:14][C:15]([O-:17])=[O:16].[NH2:2][C@H:3]([C:9]([OH:11])=[O:10])[CH2:4][CH2:5][CH2:6][CH2:7][NH2:8].[NH2:2][C@H:3]([C:9]([OH:11])=[O:10])[CH2:4][CH2:5][CH2:6][CH2:7][NH2:8].[Na+:20].[Na+:20]

参加物

6

反応物 4

HCID 313Hydrochloric Acid2 回HCID 1110Succinic AcidHCID 9020Sodium SuccinateHCID 16211825Lysine Monohydrate

生成物 1

HCID 86749085Sodium Dilysine Succinate Hydrochloride

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

12 grams of L-lysine monohydrate is dissolved in 20 ml of water to which 6.0 ml of concentrated hydrochloric acid has been added. 2.964 grams of disodium succinate is added to neutralize some of the excess hydrochloric acid and 2.16 grams of succinic acid are added with mixing until effervescence ceases and all solids are dissolved. The solution is dried in a 110° C. oven until solids begin to form when cooled to room temperature. After 15 to 30 minutes solids form and are collected.

後処理

  1. additionhas been added
  2. additionare added
  3. additionwith mixing until effervescence ceases
  4. dissolutionall solids are dissolved
  5. customThe solution is dried in a 110° C. oven until solids
  6. customto form when
  7. customare collected

出典と根拠

ORDレコード
ord-339483346657436b902a53b436f4e6f4
出典データセット
uspto-grants-1997_04
特許番号
US05618467

関連ノート

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