反応式
[CH2:1]([NH:8][CH:9]=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[S-:11][C:12]#[N:13].[Na+:14]>>[CH2:1]([NH:8][CH:9]=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[S-:11][C:12]#[N:13].[Na+:14]参加物
3
反応条件
- 温度
- 30 °C
実験手順
To a round-bottom flask, 9.9 g of purified N-benzyl formamide and 4 g of NaSCN (sodium thiocyanate) were introduced. The mixture was agitated gradually under nitrogen atmosphere at 30° C. for 40 minutes, and then at room temperature for 5 hours to obtain 10.7 g of N-benzyl formamide-NaSCN eutectic mixture.
出典と根拠
- ORDレコード
- ord-92c554d1877b4115a46c924621464c74
- 出典データセット
- uspto-grants-2014_10
- 特許番号
- US08858837B2
関連ノート
読み込み中…